Rapid confirmatory analysis of avermectin residues in milk by liquid chromatography tandem mass spectrometry

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dc.authorscopusid56988763200
dc.authorscopusid6602622021
dc.contributor.authorÖzdemir, Nurullah
dc.contributor.authorKahraman, Tahir
dc.date.accessioned2022-05-11T14:42:18Z
dc.date.available2022-05-11T14:42:18Z
dc.date.issued2016
dc.departmentFakülteler, Veteriner Fakültesi, Klinik Öncesi Bilimler Bölümü, Farmakoloji ve Toksikoloji Ana Bilim Dalı
dc.description.abstractOur study developed a quick method for confirmatory analysis of avermectins (abamectin B1a, doramectin, ivermectin B1a, eprinomectin B1a, and moxidectin) in bovine milk according to the European Commission Decision 2002/657/EC requirements. Avermectins were liquid-liquid extracted with acetonitrile, followed by an evaporation step, and then analyzed by liquid chromatography/electrospray ionization tandem mass spectrometry in the negative ion mode. An in-house method validation was performed and the data reported on specificity, linearity, recovery, limit of detection, limit of quantitation, decision limit, and detection capability. The advantage of this method is that low levels of avermectins are detectable and quantitatively confirmed at a rapid rate in milk. © 2015, Food and Drug Administration, Taiwan. Published by Elsevier Taiwan LLC.
dc.identifier.doi10.1016/j.jfda.2015.07.004
dc.identifier.endpage94
dc.identifier.issn1021-9498
dc.identifier.issue1en_US
dc.identifier.scopus2-s2.0-84957429350
dc.identifier.scopusqualityQ1
dc.identifier.startpage90
dc.identifier.urihttps://doi.org/10.1016/j.jfda.2015.07.004
dc.identifier.urihttps://hdl.handle.net/20.500.11776/9323
dc.identifier.volume24
dc.indekslendigikaynakScopus
dc.institutionauthorÖzdemir, Nurullah
dc.language.isoen
dc.publisherElsevier Taiwan LLC
dc.relation.ispartofJournal of Food and Drug Analysis
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/openAccess
dc.subjectavermectin
dc.subjectliquid chromatography/tandem mass spectrometry
dc.subjectmilk
dc.subjectresidue
dc.subjectabamectin b1a
dc.subjectacetonitrile
dc.subjectavermectin derivative
dc.subjectdoramectin
dc.subjecteprinomectin b1a
dc.subjectivermectin b1a
dc.subjectmoxidectin
dc.subjectunclassified drug
dc.subjectArticle
dc.subjectbovine
dc.subjectelectrospray
dc.subjectevaporation
dc.subjectlimit of detection
dc.subjectlimit of quantitation
dc.subjectliquid chromatography
dc.subjectliquid liquid extraction
dc.subjectmilk
dc.subjectnonhuman
dc.subjectquantitative study
dc.subjecttandem mass spectrometry
dc.subjectvalidation study
dc.titleRapid confirmatory analysis of avermectin residues in milk by liquid chromatography tandem mass spectrometry
dc.typeArticle

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