Rapid confirmatory analysis of avermectin residues in milk by liquid chromatography tandem mass spectrometry
Yükleniyor...
Dosyalar
Tarih
2016
Yazarlar
Dergi Başlığı
Dergi ISSN
Cilt Başlığı
Yayıncı
Elsevier Taiwan LLC
Erişim Hakkı
info:eu-repo/semantics/openAccess
Özet
Our study developed a quick method for confirmatory analysis of avermectins (abamectin B1a, doramectin, ivermectin B1a, eprinomectin B1a, and moxidectin) in bovine milk according to the European Commission Decision 2002/657/EC requirements. Avermectins were liquid-liquid extracted with acetonitrile, followed by an evaporation step, and then analyzed by liquid chromatography/electrospray ionization tandem mass spectrometry in the negative ion mode. An in-house method validation was performed and the data reported on specificity, linearity, recovery, limit of detection, limit of quantitation, decision limit, and detection capability. The advantage of this method is that low levels of avermectins are detectable and quantitatively confirmed at a rapid rate in milk. © 2015, Food and Drug Administration, Taiwan. Published by Elsevier Taiwan LLC.
Açıklama
Anahtar Kelimeler
avermectin, liquid chromatography/tandem mass spectrometry, milk, residue, abamectin b1a, acetonitrile, avermectin derivative, doramectin, eprinomectin b1a, ivermectin b1a, moxidectin, unclassified drug, Article, bovine, electrospray, evaporation, limit of detection, limit of quantitation, liquid chromatography, liquid liquid extraction, milk, nonhuman, quantitative study, tandem mass spectrometry, validation study
Kaynak
Journal of Food and Drug Analysis
WoS Q Değeri
Scopus Q Değeri
Q1
Cilt
24
Sayı
1
