Poly(9H-Carbazole-9-Carbothioic Dithioperoxyanhydride) Formation and Capacitor Study

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dc.authorid0000-0002-1806-0330
dc.authorid0000-0002-2819-3612
dc.authorscopusid9735216100
dc.authorscopusid6507868758
dc.authorwosiduludag, Nesimi/AAB-1353-2020
dc.authorwosidAtes, Murat/G-3798-2012
dc.contributor.authorAteş, Murat
dc.contributor.authorUludağ, Nesimi
dc.date.accessioned2022-05-11T14:30:52Z
dc.date.available2022-05-11T14:30:52Z
dc.date.issued2015
dc.departmentFakülteler, Fen Edebiyat Fakültesi, Kimya Bölümü
dc.description.abstract9H-Carbazole-9-carbothioic dithioperoxyanhydride (2CS(2)Cz) was chemically synthesized in our previous study. In this work, specific (C-sp) and double layer capacitances (C-dl) of the electrocoated poly(9H-carbazole-9-carbothioic dithioperoxyanhydride) P(2CS(2)Cz) films were obtained on glassy carbon electrode (GCE). The polymers were characterized by cyclic voltammetry (CV), Fourier transform infrared reflectance-attenuated total reflection spectroscopy (FTIR-ATR), scanning electron microscopy (SEM), energy dispersive X-ray analysis (EDX), and electrochemical impedance spectroscopy (EIS). Polymer characterizations of FTIR-ATR, and SEM-EDX analysis were taken on carbon fiber microelectrodes (CFMEs). The initial monomer concentration of 2CS(2)Cz was taken as 0.25, 0.5, and 1.0mM in 0.1M sodium perchlorate (NaClO4)/acetonitrile (CH3CN). The capacitance behavior of P(2CS(2)Cz)/GCE is shown by Nyquist, Bode-magnitude, Bode-phase, and Admittance plots relationship. The low frequency capacitance (C-LF=0.52 mFcm(-2)) and double layer capacitance (C-dl=571 mu F) were obtained for [2CS(2)Cz](0)=0.25mM and 1mM, respectively. [GRAPHICS] .
dc.identifier.doi10.1080/00914037.2014.1002133
dc.identifier.endpage761
dc.identifier.issn0091-4037
dc.identifier.issn1563-535X
dc.identifier.issue14en_US
dc.identifier.scopus2-s2.0-84928195145
dc.identifier.scopusqualityQ2
dc.identifier.startpage755
dc.identifier.urihttps://doi.org/10.1080/00914037.2014.1002133
dc.identifier.urihttps://hdl.handle.net/20.500.11776/7205
dc.identifier.volume64
dc.identifier.wosWOS:000352801700006
dc.identifier.wosqualityQ2
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.institutionauthorAteş, Murat
dc.institutionauthorUludağ, Nesimi
dc.language.isoen
dc.publisherTaylor & Francis As
dc.relation.ispartofInternational Journal of Polymeric Materials and Polymeric Biomaterials
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.subjectCapacitance
dc.subjectconducting polymer
dc.subjectelectrochemical impedance spectroscopy
dc.subjectelectropolymerization
dc.subjectpoly(2CS(2)Cz)
dc.subjectElectrochemical Impedance Spectroscopy
dc.subjectCarbon-Fiber
dc.subjectElectropolymerization
dc.subjectMorphology
dc.subjectCorrosion
dc.subjectPolycarbazoles
dc.subjectMethacrylate)
dc.subjectElectrolyte
dc.subjectPerformance
dc.subjectBehavior
dc.titlePoly(9H-Carbazole-9-Carbothioic Dithioperoxyanhydride) Formation and Capacitor Study
dc.typeArticle

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