Determination of Major, Minor, and Toxic Elements in Tropical Fruits by ICP-OES After Different Microwave Acid Digestion Methods

Basit Öğe Kaydı
dc.authorscopusid55235059200
dc.contributor.authorKarasakal, Ayça
dc.date.accessioned2022-05-11T14:31:05Z
dc.date.available2022-05-11T14:31:05Z
dc.date.issued2021
dc.departmentFakülteler, Fen Edebiyat Fakültesi, Kimya Bölümü
dc.description.abstractFruits contain nutrients, minerals, trace elements, vitamins, and phytochemicals that are important in terms of human health. When fruits are consumed in a balanced diet, they have a positive effect with regard to reducing disease risk. As a result of heavy metal contamination of the environment, they can be a potential source of toxic elements so it is important to determine the toxic, essential, and trace elements in fresh fruit and commercial fruit products such as fruit juice, marmalade. This study aims to determine the concentrations of Al, B, Ca, Cu, Fe, K, Mg, Mn, Na, Zn, P, and S in tropical fruits (tamarind (Tamarindus indica), star fruit (Averrhoa carambola), golden berry (Physalis peruviana), kumquat (Citrus japonica), dragon fruit (Hylocereus undatus), passion fruit (Passiflora edulis)) by using inductively coupled plasma optical emission spectrometry (ICP-OES) after different microwave acid digestion procedures. The efficiencies of digestion in tropical fruit samples were investigated and compared. Six milliliters of HNO3 + 2 mL of H2O2, 6 mL of HNO3 + 2 mL of HCl, 8 mL of HNO3, 8 mL of HNO3 + 4 mL of H2O2(30%), 8 mL of HNO3 + 4 mL of HCl, and 12 mL of HNO(3)were used for microwave acid digestion procedures. Microwave digestion procedures were applied for the analysis of seventy-two tropical fruit samples purchased in triplicate for each tropical fruit and major, toxic, and minor element contents of tropical fruits were determined. The parameters of the merit evaluated were validated according to limits of detection (LOD) and limits of quantification (LOQ), linearity, recovery, and precision. The highest results of LOD and LOQ were found for Ca, K, Na, Mg, and S. The recovery percentages are in the range from 71.01 to 117.31% in tropical fruits. The digestion efficiency was correlated with the residual carbon content, which was determined by total organic carbon analyzer (TOC). Six milliliters of HNO3 + 2 mL of HCl digestion method was chosen as the effective digestion method because of the lowest residual carbon contents and the accuracy results.
dc.description.sponsorshipResearch Fund of the University of Namik Kemal UniversityNamik Kemal University; NKUBAP [16.026]
dc.description.sponsorshipThis study was supported by the Research Fund of the University of Namik Kemal University (Project Number: NKUBAP. 00.GA.16.026).
dc.identifier.doi10.1007/s12161-020-01884-3
dc.identifier.endpage360
dc.identifier.issn1936-9751
dc.identifier.issn1936-976X
dc.identifier.issue2en_US
dc.identifier.scopus2-s2.0-85092701869
dc.identifier.scopusqualityQ2
dc.identifier.startpage344
dc.identifier.urihttps://doi.org/10.1007/s12161-020-01884-3
dc.identifier.urihttps://hdl.handle.net/20.500.11776/7315
dc.identifier.volume14
dc.identifier.wosWOS:000579609700003
dc.identifier.wosqualityQ2
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.institutionauthorKarasakal, Ayça
dc.language.isoen
dc.publisherSpringer
dc.relation.ispartofFood Analytical Methods
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.subjectGolden berry
dc.subjectPassion fruit
dc.subjectTamarind
dc.subjectDragon fruit
dc.subjectKumquat
dc.subjectStar fruit
dc.subjectDiluted Nitric-Acid
dc.subjectAssisted Digestion
dc.subjectTrace-Elements
dc.subjectMetals
dc.subjectMs
dc.subjectBiodiesel
dc.subjectCalcium
dc.subjectSodium
dc.subjectJuices
dc.subjectOxygen
dc.titleDetermination of Major, Minor, and Toxic Elements in Tropical Fruits by ICP-OES After Different Microwave Acid Digestion Methods
dc.typeArticle

Dosyalar

Orijinal paket
Listeleniyor 1 - 1 / 1
Küçük Resim Yok
İsim:
7315.pdf
Boyut:
649.92 KB
Biçim:
Adobe Portable Document Format
Açıklama:
Tam Metin / Full Text
İndir

Koleksiyon

WoS İndeksli Yayınlar Koleksiyonu
Fen Edebiyat Fakültesi Koleksiyonu
Scopus İndeksli Yayınlar Koleksiyonu