Synthesis, photophysical and antioxidant properties of carbazole-based bis-thiosemicarbazones

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dc.authorid0000-0001-9386-4892
dc.authorid0000-0002-3579-8062
dc.authorid0000-0002-7347-2223
dc.authorid0000-0003-4163-9962
dc.authorscopusid26029066300
dc.authorscopusid34168278000
dc.authorscopusid57201682024
dc.authorscopusid35866927300
dc.authorscopusid55326408200
dc.authorscopusid55308985300
dc.authorwosidSengul, Ibrahim Fazil/AAG-4368-2019
dc.authorwosidŞenkuytu, Elif/ABI-5315-2020
dc.authorwosidk, h/ABA-1339-2020
dc.authorwosidsaglam, mehmet/Y-7456-2019
dc.contributor.authorBingül, Murat
dc.contributor.authorŞenkuytu, Elif
dc.contributor.authorSağlam, Mehmet Turgut
dc.contributor.authorBoga, Mehmet
dc.contributor.authorKandemir, Hakan
dc.contributor.authorŞengül, İbrahim Fazıl
dc.date.accessioned2022-05-11T14:31:03Z
dc.date.available2022-05-11T14:31:03Z
dc.date.issued2019
dc.departmentFakülteler, Fen Edebiyat Fakültesi, Kimya Bölümü
dc.description.abstractUtilizing Schiff base condensation of the 9-ethylcarbazole-3,6-dicarbaldehyde and thiosemicarbazides, four new N-ethylcarbazole-based bis-thiosemicarbazone compounds 4a-d were successfully synthesized in high yields. The photophysical properties of the targeted compounds 4a-d were investigated using UV-vis absorption and fluorescence emission spectroscopy. The antioxidant properties of targeted compounds 4a-d were determined by DPPH radical scavenging, ABTS Cation Radical Decolarization and CUPRAC Cupric Reducing Antioxidant Capacity assay methods. Moreover, the anti-cholinesterase properties of designated compounds were investigated by the Acetylcholinesterase (Ach) and Butyrylcholinesterase (BCh) enzyme inhibition assays. The compound 4a was determined as a valuable candidate to be a potent antioxidant agent for the DPPH and ABTS assays. The compound 4d was found to be a target compound for the kinetic measurements to identify the mechanism of action in the area of anticholinesterase activity assay.
dc.description.sponsorshipDicle University Scientific Research Project Coordinator (DUBAP Project)Dicle University [ECZ 15.007]
dc.description.sponsorshipI thank the Dicle University Scientific Research Project Coordinator (DUBAP Project Number: ECZ 15.007) for the financial support given to the research project.
dc.identifier.doi10.1007/s11164-019-03844-x
dc.identifier.endpage4499
dc.identifier.issn0922-6168
dc.identifier.issn1568-5675
dc.identifier.issue9en_US
dc.identifier.scopus2-s2.0-85065244657
dc.identifier.scopusqualityQ2
dc.identifier.startpage4487
dc.identifier.urihttps://doi.org/10.1007/s11164-019-03844-x
dc.identifier.urihttps://hdl.handle.net/20.500.11776/7293
dc.identifier.volume45
dc.identifier.wosWOS:000481805000016
dc.identifier.wosqualityQ3
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.institutionauthorKandemir, Hakan
dc.language.isoen
dc.publisherSpringer
dc.relation.ispartofResearch on Chemical Intermediates
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.subjectCarbazole
dc.subjectThiosemicarbazone
dc.subjectAntioxidant activities
dc.subjectPhotophysical properties
dc.subjectLigand Synthesis
dc.subjectFluorescence
dc.subjectDerivatives
dc.subjectCopper(Ii)
dc.subjectComplexes
dc.subjectIron
dc.titleSynthesis, photophysical and antioxidant properties of carbazole-based bis-thiosemicarbazones
dc.typeArticle

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