Adsorption of industrial Acid Red 114 onto Fe3O4@ Histidine magnetic nanocomposite

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dc.authorid0000-0001-5853-4126
dc.authorid0000-0002-1457-1504
dc.authorid0000-0002-5205-0937
dc.authorscopusid55234742700
dc.authorscopusid14522763100
dc.authorscopusid56432454500
dc.authorscopusid7005225253
dc.authorwosidYıldız, Aylin/ABA-6155-2020
dc.authorwosidAmir/D-8880-2015
dc.authorwosidBaykal, Abdulhadi/AAF-9826-2019
dc.authorwosidGüneş, Elçin/ABA-1276-2020
dc.authorwosidGüneş, Elçin/ABA-2259-2020
dc.contributor.authorYıldız, Aylin
dc.contributor.authorGüneş, Elçin
dc.contributor.authorAmir, M. D.
dc.contributor.authorBaykal, Abdulhadi
dc.date.accessioned2022-05-11T14:10:30Z
dc.date.available2022-05-11T14:10:30Z
dc.date.issued2017
dc.departmentFakülteler, Çorlu Mühendislik Fakültesi, Tekstil Mühendisliği Bölümü
dc.departmentFakülteler, Çorlu Mühendislik Fakültesi, Çevre Mühendisliği Bölümü
dc.description.abstractFe3O4@ Histidine (Fe3O4@ His) magnetic nanocomposite (MNCs) was successfully prepared by simple thermal decomposition method. The final obtained products were characterized by X-ray diffraction (XRD), Fourier transform infrared (FT-IR), thermogravimetric analysis, scanning electron microscope (SEM), and transmission electron microscopy (TEM). Powder XRD analysis confirmed the single phase of Fe3O4 spinel structure. SEM and TEM analysis indicated that Fe3O4@ His MNCs were nanoparticles-like structure with small agglomeration. FT-IR results revealed that L-histidine made a bond through its COO-group with Fe3O4 Nanoparticles (NPs). There is electrostatic attraction between cationic NH2 group (NH3+) of Fe3O4@ His MNCs and anionic dye. The Fe3O4@ His MNC has much higher adsorbed amount of Acid Red 114 (AR114) than the Fe3O4 NPs at pH 5 and 8. At pH -5 on the nanoparticle surface via ammonium groups. Thermal analysis showed the decomposition of the L-histidine capping. The hysteresis (sigma-H) curves revealed Fe3O4@ His MNC exhibit a typical super paramagnetic characteristic with a saturation magnetization of 45.5 emu/g. The adsorption capacity of low-cost and eco-friendly adsorbents Fe3O4@ His nanocomposite for removal of industrial AR114 from wastewater was investigated. Therefore, pH of 5 and contact time of 120 min were found to be optimum for maximum removal of AR114 by Fe3O4@ His MNCs. The experimental data of adsorption obey Langmuir isotherm and pseudo-second-order kinetic. The maximum adsorption capacity of the Fe3O4@ His MNC for AR114 was 140.8 mg/g at pH 5. The reusability of the Fe3O4@ His MNCs was also done, and significant removal of AR114 obtained even after five cycles. Thus, Fe3O4@ His MNCs considered as a good stability and reusability absorbent for the removal of industrial AR114.
dc.description.sponsorshipFatih University Research office [P50031504_B (10790)]
dc.description.sponsorshipThis study was supported by Fatih University Research office with the project number: P50031504_B (10790).
dc.identifier.doi10.5004/dwt.2017.0295
dc.identifier.endpage268
dc.identifier.issn1944-3994
dc.identifier.issn1944-3986
dc.identifier.scopus2-s2.0-85020239731
dc.identifier.scopusqualityQ3
dc.identifier.startpage261
dc.identifier.urihttps://doi.org/10.5004/dwt.2017.0295
dc.identifier.urihttps://hdl.handle.net/20.500.11776/5422
dc.identifier.volume60
dc.identifier.wosWOS:000403564800025
dc.identifier.wosqualityQ3
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.institutionauthorYıldız, Aylin
dc.institutionauthorGüneş, Elçin
dc.language.isoen
dc.publisherDesalination Publ
dc.relation.ispartofDesalination and Water Treatment
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.subjectWastewater treatment
dc.subjectMagnetic nanocomposite
dc.subjectAdsorption
dc.subjectAcid Red 114
dc.subjectRecyclable Nanocatalyst
dc.subjectAqueous-Solution
dc.subjectMethylene-Blue
dc.subjectAzo Dyes
dc.subjectRemoval
dc.subjectNanoparticles
dc.subjectWater
dc.subjectDegradation
dc.subjectEquilibrium
dc.subjectReduction
dc.titleAdsorption of industrial Acid Red 114 onto Fe3O4@ Histidine magnetic nanocomposite
dc.typeArticle

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