Determination of sulfonamides in milk by ID-LC-MS/MS

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dc.authorid0000-0002-5470-130X
dc.authorwosidAydın, Ebru/D-1403-2010
dc.authorwosidtasan, murat/ABA-3434-2020
dc.authorwosidGoren, Ahmet C/G-1562-2017
dc.contributor.authorAydın Ünsal, Işın
dc.contributor.authorTaşan, Murat
dc.contributor.authorGökçen, Taner
dc.contributor.authorGören, Ahmet C.
dc.date.accessioned2022-05-11T14:44:57Z
dc.date.available2022-05-11T14:44:57Z
dc.date.issued2018
dc.departmentFakülteler, Ziraat Fakültesi, Gıda Mühendisliği Bölümü
dc.description.abstractIn this study, an ID-LC-MS method was developed and validated for the determination of 14 sulfonamides in milk samples. Recovery results were found to be in the range of 91%-114% for milk samples. The relative measurement uncertainty was between 7.5%-12.7%. Validated method was performed on milk samples obtained from market and street vendors. The amount of sulfonamides in the analyzed samples was found to be below the legal limits (Sulfamethazine: 6.46 +/- 0.76 ng/g and sulfisoxazole: 7.3 +/- 0.71 ng/g).
dc.identifier.doi10.25135/jcm.15.18.04.081
dc.identifier.endpage78
dc.identifier.issn1307-6183
dc.identifier.issue1en_US
dc.identifier.startpage70
dc.identifier.urihttps://doi.org/10.25135/jcm.15.18.04.081
dc.identifier.urihttps://hdl.handle.net/20.500.11776/9847
dc.identifier.volume12
dc.identifier.wosWOS:000436246200006
dc.identifier.wosqualityN/A
dc.indekslendigikaynakWeb of Science
dc.institutionauthorAydın Ünsal, Işın
dc.institutionauthorTaşan, Murat
dc.language.isoen
dc.publisherAcg Publications
dc.relation.ispartofJournal of Chemical Metrology
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/openAccess
dc.subjectSulfonamides
dc.subjectisotope dilution
dc.subjectLC-MS/MS
dc.subjectmethod validation
dc.subjectuncertainty estimation
dc.subjectTandem Mass-Spectrometry
dc.subjectPerformance Liquid-Chromatography
dc.subjectSolid-Phase Extraction
dc.subjectModified Quechers
dc.subjectVeterinary Drugs
dc.subjectResidues
dc.subjectValidation
dc.subjectSamples
dc.subjectProducts
dc.subjectMicroextraction
dc.titleDetermination of sulfonamides in milk by ID-LC-MS/MS
dc.typeArticle

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