A novel synthesis of 3,6-bis(2,3-dihydrothieno[3,4-b][1,4]dioxin-5-yl)-9-tosyl-9H-carbazole

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dc.authorid0000-0002-1806-0330
dc.authorwosidAtes, Murat/G-3798-2012
dc.authorwosiduludag, Nesimi/AAB-1353-2020
dc.contributor.authorAteş, Murat
dc.contributor.authorUludağ, Nesimi
dc.contributor.authorKarazehir, Tolga
dc.contributor.authorArican, Fatih
dc.date.accessioned2022-05-11T14:29:46Z
dc.date.available2022-05-11T14:29:46Z
dc.date.issued2012
dc.departmentFakülteler, Fen Edebiyat Fakültesi, Kimya Bölümü
dc.description.abstract3,6-bis(2,3-dihydrothieno [3,4-b][1,4]dioxin-5-yl)-9-tosyl-9H-carbazole (EDOTTsCz) was synthesized and electrochemically polymerized on glassy carbon electrode (GCE) in 0.1 M tetrabutyl ammonium tetrafluoroborate (NB4BF4)/acetonitrile (CH3CN). Alternating copolymer was formed by CV method. Modified polymer electrode was characterized by Fourier transform Infrared Spectroscopy-Attenuated Transmission Reflectance (FTIR-ATR), Cyclic voltammetry (CV), Scanning electron microscopy-Energy dispersive X-ray analysis (SEM-EDX), Atomic force microscope (AFM) and Electrochemical impedance spectroscopy (EIS). Capacitive behaviors of the modified GCE were defined via Nyquist, Bode-magnitude, Bode-phase and Capacitance plots. A modified copolymer electrode provides enhanced capacitance evaluation, which may results in performance in energy storage devices.
dc.description.sponsorshipTUBITAK (Scientific and Technological Reseach Council of Turkey) [110T791]
dc.description.sponsorshipThe support of the TUBITAK (Scientific and Technological Reseach Council of Turkey) (110T791) is gratefully acknowledged. We also thank to Serhat Tikiz (Afyon Kocatepe University, Technology and Research Center, (TUAM), Afyon, Turkey) and Yakup Bakis (Fatih University, BINATAM, Istanbul, Turkey) for recording SEMEDX and AFM images, respectively.
dc.identifier.doi10.2478/v10310-012-0010-9
dc.identifier.endpage71
dc.identifier.issn1583-2430
dc.identifier.issn2286-038X
dc.identifier.issue1en_US
dc.identifier.startpage63
dc.identifier.urihttps://doi.org/10.2478/v10310-012-0010-9
dc.identifier.urihttps://hdl.handle.net/20.500.11776/7125
dc.identifier.volume23
dc.identifier.wosWOS:000219328500010
dc.identifier.wosqualityN/A
dc.indekslendigikaynakWeb of Science
dc.institutionauthorAtes, Murat
dc.institutionauthorUludağ, Nesimi
dc.institutionauthorKarazehir, Tolga
dc.institutionauthorArican, Fatih
dc.language.isoen
dc.publisherOvidius Univ Press
dc.relation.ispartofOvidius University Annals of Chemistry
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/openAccess
dc.subjectCopolymer
dc.subjectCapacitance
dc.subjectScanning electron microscopy (SEM)
dc.subjectAtomic force microscopy (AFM)
dc.titleA novel synthesis of 3,6-bis(2,3-dihydrothieno[3,4-b][1,4]dioxin-5-yl)-9-tosyl-9H-carbazole
dc.typeArticle

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