Ara
Toplam kayıt 10, listelenen: 1-10
The synthesis and spectroscopic characterization of (+)-demethoxyaspidospermine: Density functional theory calculations of the structural, electronic, and non-linear optic and spectroscopic properties
(SAGE Publications Ltd, 2019)
(+)-Demethoxyaspidospermine was synthesized via the acylation of aspidospermidine with acetic anhydride, and the structure was determined by elemental analysis and Fourier-transform infrared and nuclear magnetic resonance ...
A new approach to the total synthesis of (±)-nordasycarpidone by ring-closure with tetrachloro-1,4-benzoquinone
(Macedonian Journal of Chemistry and Chemical Engineering, 2020)
new synthetic route for the (±)-nordasycarpidone was achieved in five steps with an overall yield of 41 %. This route involves ring closure and formation of 5 which has a methanoazocino[4,3-b]indole skeleton in the key ...
Reactions of Methyl Acetylenecarboxylate with Heterocyclic Enamines: [2+2] Cycloadditions in Polar and Non-Polar Solvents
(Asian Journal Of Chemistry, 2014)
In this study, enamines of cyclic ketones reacting with methyl acetylenecarboxylate to produce intermadiate cyclobutene adducts have been isolated. Reactions of methyl acetylenecarboxylate with enamines derived from ...
9-(4-Nitrophenylsulfonyl)-9H-carbazole
(Wiley-Blackwell, 2011)
In the title molecule, C18H12N2O4S, the carbazole skeleton is nearly planar [maximum deviation = 0.037 (1) A] and is oriented at a dihedral angle of 73.73 (5)degrees with respect to the benzene ring. An intramolecular ...
Synthesis of methyl 4-(9H-carbazole-9-carbanothioylthio) benzoate: electropolymerization and impedimetric study
(Scientific Technical Research Council Turkey-Tubitak, 2015)
Methyl 4((9H-(carbazole-97carbanothioylthio) benzoate (MCzCTB) was chemically synthesized and characterized by FTIR, H-1 NMR, and C-13 NMR. A novel synthesized monomer was electropolymerized on a glassy carbon electrode ...
A novel synthesis of 4-toluene 9H-carbazole-9-carbodithioate, electropolymerization and impedance study
(Budapest Univ Technol & Econ, 2014)
A novel synthesis of 4-toluene 9H-carbazole-9-carbodithioate (TCzC) was chemically synthesized and characterized by Fourier Transform Infrared (FTIR), proton nuclear magnetic resonance (H-1-NMR), and carbon nuclear magnetic ...
New route for synthesis of 2-(2,2-dimethoxyethyl)-1,2,3,4,5,6-hexahydro-1,5-methanoazocino[4,3-b] indole and DFT investigation
(Elsevier Sci Ltd, 2020)
Development of efficient sequences for the synthesis of the title compound (2-(2,2-dimethoxyethyl)-1,2,3,4,5,6-hexahydro-1,5-methanoazocino[4,3-b]indole) (7) was described. The title compound was synthesized through several ...
A new reagent for efficient synthesis of nitriles from aldoximes using methoxymethyl bromide
(Editura Academiei Romane, 2021)
This study outlines an efficient, high-yielding, and rapid method by which to access diverse nitriles from aldoximes with methoxymethyl bromide (MOM-Br) in THF. It represents the first application of MOM-Br as a deoximation ...
Strychnos alkaloids: total synthesis, characterization, DFT investigations, and molecular docking with AChE, BuChE, and HSA
(Elsevier Sci Ltd, 2022)
An efficient five steps, the protection-deprotection synthetic a novel synthetic routes to(+/-) noruleine (f)-uleine, are reported starting from tetrahydrocarbazole fused monoalkyl nitrile at C-2 position that is prepared ...
A SIMPLE AND EFFICIENT METHOD FOR CONSTRUCTING AZOCINO[4,3-b]INDOLE
(Macedonian Journal of Chemistry and Chemical Engineering, 2022)
A new synthetic procedure has been developed to prepare the biologically important azocino[4,3-b]indole via the tetrafluoro-1,4-benzoquinone (TFB)-mediated cyclization of a tetrahydrocarbazole derivative bearing an amide ...