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Determination of sulfonamides in milk by ID-LC-MS/MS

dc.contributor.authorAydın Ünsal, Işın
dc.contributor.authorTaşan, Murat
dc.contributor.authorGökçen, Taner
dc.contributor.authorGören, Ahmet C.
dc.date.accessioned2022-05-11T14:44:57Z
dc.date.available2022-05-11T14:44:57Z
dc.date.issued2018
dc.identifier.issn1307-6183
dc.identifier.urihttps://doi.org/10.25135/jcm.15.18.04.081
dc.identifier.urihttps://hdl.handle.net/20.500.11776/9847
dc.description.abstractIn this study, an ID-LC-MS method was developed and validated for the determination of 14 sulfonamides in milk samples. Recovery results were found to be in the range of 91%-114% for milk samples. The relative measurement uncertainty was between 7.5%-12.7%. Validated method was performed on milk samples obtained from market and street vendors. The amount of sulfonamides in the analyzed samples was found to be below the legal limits (Sulfamethazine: 6.46 +/- 0.76 ng/g and sulfisoxazole: 7.3 +/- 0.71 ng/g).en_US
dc.language.isoengen_US
dc.publisherAcg Publicationsen_US
dc.identifier.doi10.25135/jcm.15.18.04.081
dc.rightsinfo:eu-repo/semantics/openAccessen_US
dc.subjectSulfonamidesen_US
dc.subjectisotope dilutionen_US
dc.subjectLC-MS/MSen_US
dc.subjectmethod validationen_US
dc.subjectuncertainty estimationen_US
dc.subjectTandem Mass-Spectrometryen_US
dc.subjectPerformance Liquid-Chromatographyen_US
dc.subjectSolid-Phase Extractionen_US
dc.subjectModified Quechersen_US
dc.subjectVeterinary Drugsen_US
dc.subjectResiduesen_US
dc.subjectValidationen_US
dc.subjectSamplesen_US
dc.subjectProductsen_US
dc.subjectMicroextractionen_US
dc.titleDetermination of sulfonamides in milk by ID-LC-MS/MSen_US
dc.typearticleen_US
dc.relation.ispartofJournal of Chemical Metrologyen_US
dc.departmentFakülteler, Ziraat Fakültesi, Gıda Mühendisliği Bölümüen_US
dc.authorid0000-0002-5470-130X
dc.identifier.volume12en_US
dc.identifier.issue1en_US
dc.identifier.startpage70en_US
dc.identifier.endpage78en_US
dc.institutionauthorAydın Ünsal, Işın
dc.institutionauthorTaşan, Murat
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.authorwosidAydın, Ebru/D-1403-2010
dc.authorwosidtasan, murat/ABA-3434-2020
dc.authorwosidGoren, Ahmet C/G-1562-2017
dc.identifier.wosWOS:000436246200006en_US


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