The electropolymerization of N,N-(propane-1,3-diyl)bis(2-aminobenzamide), characterization, and capacitor study

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dc.authorid0000-0002-1806-0330
dc.authorscopusid9735216100
dc.authorscopusid7801447801
dc.authorscopusid57190170387
dc.authorscopusid16241035900
dc.authorwosidAtes, Murat/G-3798-2012
dc.contributor.authorAteş, Murat
dc.contributor.authorKolancilar, Hakan
dc.contributor.authorÇalışkan, Sinan
dc.contributor.authorÇınar, Damla
dc.date.accessioned2022-05-11T14:31:00Z
dc.date.available2022-05-11T14:31:00Z
dc.date.issued2018
dc.departmentFakülteler, Fen Edebiyat Fakültesi, Kimya Bölümü
dc.description.abstractIn this study, aniline-based monomer, N,N-(propane-1,3-diyl)bis(2-aminobenzamide), (PAB), was synthesized and characterized by proton nuclear magnetic resonance (1H-NMR), carbon-13 nuclear magnetic resonance (13C-NMR), and Fourier transform infrared spectroscopy. The electropolymerization of the monomer was performed on glassy carbon electrode by cyclic voltammetry (CV). The effects of solvent, dopant, scan number, and scan rate on the electropolymerization and properties of the poly(PAB) films were investigated. The modified electrode was also characterized by Fourier transform infrared-attenuated total reflection spectroscopy and scanning electron microscopy-energy-dispersive X-ray analysis. The capacitive properties of the poly(PAB) films were firstly tested by electrochemical impedance spectroscopy. The highest specific capacitances (C-sp) of poly(PAB) films were obtained as C-sp = 6.22 mF cm(-2) in 0.1 M lithium perchlorate/acetonitrile (ACN) for [PAB]0 = 20 mmol dm(-3) and C-sp = 16.9 mF cm(-2) in 1 mol dm(-3) sulfuric acid for [PAB]0 = 5 mmol dm(-3) at the scan rate of 5 mV s(-1) from CV measurements. This study is novel because it was the first study on capacitance performances of poly(PAB) films in the literature.
dc.identifier.doi10.1177/0954008316680279
dc.identifier.endpage93
dc.identifier.issn0954-0083
dc.identifier.issn1361-6412
dc.identifier.issue1en_US
dc.identifier.scopus2-s2.0-85040813991
dc.identifier.scopusqualityQ3
dc.identifier.startpage82
dc.identifier.urihttps://doi.org/10.1177/0954008316680279
dc.identifier.urihttps://hdl.handle.net/20.500.11776/7273
dc.identifier.volume30
dc.identifier.wosWOS:000426046900009
dc.identifier.wosqualityQ3
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.institutionauthorAteş, Murat
dc.institutionauthorÇalışkan, Sinan
dc.institutionauthorÇınar, Damla
dc.language.isoen
dc.publisherSage Publications Ltd
dc.relation.ispartofHigh Performance Polymers
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.subjectCoatings
dc.subjectcapacitance
dc.subjectelectrochemical impedance spectroscopy
dc.subjectpseudocapacitance
dc.subjectelectropolymerization
dc.subjectOptical-Properties
dc.subjectHigh-Performance
dc.subjectCarbon Materials
dc.subjectPolyaniline
dc.subjectImpedance
dc.subjectGraphene
dc.subjectFiber
dc.subjectNanocomposites
dc.subjectMethacrylate)
dc.subjectFabrication
dc.titleThe electropolymerization of N,N-(propane-1,3-diyl)bis(2-aminobenzamide), characterization, and capacitor study
dc.typeArticle

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